@phdthesis{Triyasmono2024,
  author    = {Triyasmono, Liling},
  title     = {Development and Application of Quantitative \(^1\)H NMR Spectroscopy and Chemometrics for Quality Determination of Red Fruit (\(Pandanus\) \(conoideus\), Lam.) Oil},
  doi       = {10.25972/OPUS-30272},
  url       = {http://nbn-resolving.de/urn:nbn:de:bvb:20-opus-302726},
  school      = {Universit{\"a}t W{\"u}rzburg},
  year      = {2024},
  abstract  = {In this thesis, a new approach of a qNMR method has been investigated to demonstrate the reliability and importance of this method as an alternative solution for analyzing oil quality parameters, especially in RFO, which has particular characteristics (red color). This study also includes the chemometric evaluation of spectral data for authentication, visual grouping, and prediction of RFO quality based on the degree of unsaturation, FFA value, and unsaturated fatty acid content. The analytical measurement procedure of NMR spectroscopy begins with optimization of the analytical acquisition parameters, including effect of solvent, effect of sample concentration, selection of appropriate internal standards, determination of T1, and method validation. Furthermore, the results of the method development were interpreted to RFO samples evaluation, which began with determining the assignment of signal spectra for the determination of AV, SV, EV, and IV simultaneously with: the hydrolysis approach and standard addition of palmitic acid.},
  subject      = {NMR-Spektroskopie},
  language  = {en}
}