TY  - JOUR
A1  - Flegler, Andreas
A1  - Schneider, Michael
A1  - Prieschl, Johannes
A1  - Stevens, Ralph
A1  - Vinnay, Thomas
A1  - Mandel, Karl
T1  - Continuous flow synthesis and cleaning of nano layered double hydroxides and the potential of the route to adjust round or platelet nanoparticle morphology
JF  - RSC Advances
N2  - Here, we report a continuous flow synthesis of nano LDH, comprising a continuous precipitation process using static mixers and followed by an immediate cleaning process via a semi-continuous centrifuge to obtain the final product in one-go. Via this synthesis setup, it is possible to independently vary the concentrations of the reactants during precipitation and at the same time ensure constant reaction conditions and an immediate "quenching" of the precipitate due to "on the flow"-washing. We found that this paves the way to adjust the synthesis parameters in a way that the final morphology of the nano-LDH particles can be controlled to be either round or platelet-like.
KW  - MgAl LDH
KW  - nano LDH
KW  - static mixer
KW  - synthesis process
Y1  - 2016
U6  - http://nbn-resolving.de/urn/resolver.pl?urn:nbn:de:bvb:20-opus-191305
VL  - 6
IS  - 62
ER  -