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Phase-contrast and dark-field imaging for the inspection of resin-rich areas and fiber orientation in non-crimp vacuum infusion carbon-fiber-reinforced polymers

Please always quote using this URN: urn:nbn:de:bvb:20-opus-351581
  • In this work, we present a multimodal approach to three-dimensionally quantify and visualize fiber orientation and resin-rich areas in carbon-fiber-reinforced polymers manufactured by vacuum infusion. Three complementary image modalities were acquired by Talbot–Lau grating interferometer (TLGI) X-ray microcomputed tomography (XCT). Compared to absorption contrast (AC), TLGI-XCT provides enhanced contrast between polymer matrix and carbon fibers at lower spatial resolutions in the form of differential phase contrast (DPC) and dark-field contrastIn this work, we present a multimodal approach to three-dimensionally quantify and visualize fiber orientation and resin-rich areas in carbon-fiber-reinforced polymers manufactured by vacuum infusion. Three complementary image modalities were acquired by Talbot–Lau grating interferometer (TLGI) X-ray microcomputed tomography (XCT). Compared to absorption contrast (AC), TLGI-XCT provides enhanced contrast between polymer matrix and carbon fibers at lower spatial resolutions in the form of differential phase contrast (DPC) and dark-field contrast (DFC). Consequently, relatively thin layers of resin, effectively indiscernible from image noise in AC data, are distinguishable. In addition to the assessment of fiber orientation, the combination of DPC and DFC facilitates the quantification of resin-rich areas, e.g., in gaps between fiber layers or at binder yarn collimation sites. We found that resin-rich areas between fiber layers are predominantly developed in regions characterized by a pronounced curvature. In contrast, in-layer resin-rich areas are mainly caused by the collimation of fibers by binder yarn. Furthermore, void volume around two adjacent 90°-oriented fiber layers is increased by roughly 20% compared to a random distribution over the whole specimen.show moreshow less

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Metadaten
Author: Jonathan Glinz, Jan Šleichrt, Daniel Kytýř, Santhosh Ayalur-Karunakaran, Simon Zabler, Johann Kastner, Sascha Senck
URN:urn:nbn:de:bvb:20-opus-351581
Document Type:Journal article
Faculties:Fakultät für Physik und Astronomie
Language:English
Parent Title (English):Journal of Materials Science
Year of Completion:2021
Volume:56
Issue:16
Pagenumber:9712-9727
Source:Journal of Materials Science (2021) 56:16, 9712–9727. https://doi.org/10.1007/s10853-021-05907-0
DOI:https://doi.org/10.1007/s10853-021-05907-0
Dewey Decimal Classification:5 Naturwissenschaften und Mathematik / 53 Physik / 530 Physik
Release Date:2024/06/19
Licence (German):License LogoCC BY: Creative-Commons-Lizenz: Namensnennung 4.0 International